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Pulp, paper and paperboard - Determination of sodium content

Abstract: 本文介绍了测定纸浆、纸和纸板中钠含量的步骤。首先,通过硝酸和过氧化氢消解样品,然后将消解液稀释。接着,使用火焰光度计对钠进行测定,前期需校准仪器并制备钠标准溶液。在测定过程中,将样品溶液与工作溶液混合后进行检测。最后,根据测得的钠含量和标准溶液浓度计算样品中钠的含量。文章还提醒注意样品选择、消解过程、仪器校准等,以确保测定结果的准确性和可靠性。

There are several methods for the determination of sodium in pulp, paper and board, one of the commonly used methods is as follows:

  1. Sample preparation: sample the sample to be tested according to a certain ratio, add a mixture of nitric acid and hydrogen peroxide for digestion, and then dilute the digestion solution to a certain concentration.

  2. Instrument preparation: Dilute the sodium standard solution with a concentration of 1mol/L into a working solution of a certain concentration, and use a flame photometer for preheating and calibration.

  3. Determination process: Take a certain volume of sample solution, add a certain amount of working solution and buffer solution, mix, and then use a flame photometer to measure the sodium content in the sample.

  4. Result calculation: Calculate the sodium content in the sample according to the measured sodium content of the sample and the standard solution concentration of sodium.

NBCHAO reminds you: when measuring sodium content, attention should be paid to the selection and control of the sample during the digestion process to avoid the influence of other compounds in the sample on the measurement results. At the same time, attention should be paid to the preparation and calibration of the instrument to ensure the accuracy and reliability of the measurement results.

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