There are several methods for the determination of sodium in pulp, paper and board, one of the commonly used methods is as follows:
Sample preparation: sample the sample to be tested according to a certain ratio, add a mixture of nitric acid and hydrogen peroxide for digestion, and then dilute the digestion solution to a certain concentration.
Instrument preparation: Dilute the sodium standard solution with a concentration of 1mol/L into a working solution of a certain concentration, and use a flame photometer for preheating and calibration.
Determination process: Take a certain volume of sample solution, add a certain amount of working solution and buffer solution, mix, and then use a flame photometer to measure the sodium content in the sample.
Result calculation: Calculate the sodium content in the sample according to the measured sodium content of the sample and the standard solution concentration of sodium.
NBCHAO reminds you: when measuring sodium content, attention should be paid to the selection and control of the sample during the digestion process to avoid the influence of other compounds in the sample on the measurement results. At the same time, attention should be paid to the preparation and calibration of the instrument to ensure the accuracy and reliability of the measurement results.
张维俭 - 《涂布纸及纸板生产中易出现的弊病及对策》