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Key performance detection of emulsifying agent and its method

Abstract: 乳化剂是一类能够在油水界面形成薄膜、降低界面张力以实现乳液稳定的化学物质,广泛应用于化妆品、医药、农药等领域。乳化剂的关键性能包括外观、密度、比重、折射率、溶解度、毒性、pH值、残留物、乳化能力、分散性能、稳定性、电导率和粘度。检测方法多样,如外观通过直接观察,密度和比重使用密度计和比重计,折射率通过折射仪测量,溶解度观察溶解情况,毒性通过急性毒性试验评估,pH值用酸碱滴定法或pH计法测量,残留物通过灰分法或烘干法检测。乳化能力和分散性能可通过震荡、离心、光学显微镜和动态光散射等方法评估。稳定性则通过热、冷、盐及pH值稳定性试验检验。不同乳化剂的性能测试方法需根据实际情况选择,以确保检测结果的准确性和可靠性。

An emulsifier is a chemical substance capable of uniformly mixing two immiscible liquids, such as oil and water, to form an emulsion. Emulsifiers are divided into four types: anionic, cationic, nonionic and amphoteric. Their mechanism of action is mainly to form a thin film on the oil-water interface through molecular structure, thereby reducing the tension of the oil-water interface, making the oil-water disperse and form a stable emulsifier. milky liquid. Emulsifiers are widely used in cosmetics, medicine, pesticides, coatings, food, petroleum and other fields to improve various functions and performances.

Detection performance

The following are the main properties and testing methods of common emulsifiers, as shown in the table below:

performanceDetection method
ExteriorDirectly observe the appearance of the sample
densityDensitometer method
proportionhydrometer method
Refractive indexrefractometer method
SolubilityObserve the solubility of a substance in a particular solvent
toxicityAcute Toxicity Test
pH valueAcid-base titration, pH meter method
the remainsAsh method, drying method
Emulsifying abilityShock test, centrifugal test, specific gravity test, optical microscope observation
Dispersion propertiesCentrifugal test, dynamic light scattering analysis
stabilityHeat stability test, cold stability test, salt stability test, pH value stability test
ConductivityConductivity meter method
viscosityviscometer method

NBCHAO reminds you: Different types of emulsifiers have different properties and detection methods, so it is necessary to select an appropriate detection method based on the actual situation during specific detection.

Specific detection method

The detection method of the specific emulsifier is as follows:

  1. Appearance inspection: directly observe the appearance of the sample, such as whether there is color, foreign matter, etc.

  2. Density and specific gravity testing: Use a density meter or a specific gravity meter to measure the density or specific gravity of a sample.

  3. Refractive Index Detection: Use a refractometer to measure the refractive index of a sample to assess its physical properties.

  4. Solubility Assay: Observe the solubility of a sample in a specific solvent to assess its chemical properties.

  5. Toxicity test: conduct acute toxicity test to evaluate its safety.

  6. pH value detection: Use acid-base titration or pH meter method to measure the pH value of the sample.

  7. Residue testing: Measure the residue content of a sample using the ash method or the drying method.

  8. Emulsifying ability test: conduct shock test, centrifugal test, specific gravity test, optical microscope observation and other methods to evaluate its emulsifying performance.

  9. Dispersion performance test: Centrifugal test, dynamic light scattering analysis and other methods are carried out to evaluate its dispersion performance.

  10. Stability testing: conduct heat stability test, cold stability test, salt stability test, pH value stability test and other methods to evaluate its stability performance.

  11. Conductivity detection: Use a conductivity meter to measure the conductivity of the sample.

  12. Viscosity detection: Use a viscometer to measure the viscosity of the sample.

Beichao reminds you: Different emulsifiers may require different detection methods, which should be selected according to the actual situation. At the same time, care should be taken to select appropriate instruments and equipment during testing, and operate in accordance with standard operating procedures to ensure the accuracy and reliability of testing results.

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