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Test method for platings thickness

Abstract: 本文介绍了几种测定镀层厚度的方法,强调了其在保证工件耐蚀性和导电性中的重要性。测试方法包括破坏法,如溶解法、库仑法和计时液流法,这些方法在测试过程中会破坏镀层;无损法,如磁性法、涡流法、β射线反射法和X射线荧光法,这些方法不会对镀层造成损害。此外,还有金相显微镜法、轮廓仪法等其他方法。准确选择合适的测试方法可以确保产品质量,符合相关标准能提高测试的准确性和可靠性。

The thickness of the electroplating layer is an important indicator to measure the quality of the coating, which directly affects the corrosion resistance and conductivity of the workpiece, which in turn has a significant impact on the reliability and service life of the product. Therefore, the method of accurately determining the thickness of the coating is crucial. This article will introduce various methods for testing the thickness of the coating.

1. Sabotage law

Destruction methods are a group of methods that are characterized by destroying or damaging the coating under test during testing. These methods include:

Dissolution method: This method measures the average thickness of the entire coating, dissolves the coating or base metal by soaking the sample in an appropriate solution, and then compares the weight of the sample before and after dissolution or uses chemical analysis to determine the coating quality.

Coulomb method (electricity method): The Coulomb method uses a constant DC current to pass through the electrolytic solution to dissolve the coated metal anode, and calculates the coating thickness according to the electricity consumed. This applies to the local thickness of single-layer or multi-layer single-metal coatings.

Timed flow method: Calculate the thickness of the coating by dissolving the local coating of the sample under the action of liquid flow, and then recording the time required for dissolution.

2. Non-destructive method

Nondestructive methods are a group of methods that are characterized by not destroying the coating under test during testing. These methods include:

Magnetic method: suitable for measuring the thickness of non-magnetic coatings on magnetic metal substrates. This method usually has small measurement errors, but may be slightly less accurate for thinner coatings.

Eddy current method: Using high-frequency coils to generate high-frequency magnetic fields, eddy currents are generated in the sample to be tested, and the thickness of the coating is measured according to the amplitude and phase of the eddy currents. This method is suitable for thickness measurement of non-conductive coatings on non-magnetic metal substrates.

Beta-ray reflection method: Using radioisotopes to release X-rays, the thickness of the coating is determined according to the intensity of the beta rays reflected by the tested coating. Suitable for thin precious metal coatings.

X-ray fluorescence method: By measuring the secondary X-rays generated on the metal surface, the thickness of the metal coating on the metal or non-metal substrate can be measured, and the composition of the alloy coating can also be determined.

3. Other methods

In addition to the above-mentioned destructive and non-destructive methods, there are some other methods used to measure the thickness of the coating, such as metallographic microscopy, profilometer method, interference microscopy method, double beam of light microscopy method, etc. These methods have their own advantages and applicability in specific situations, and the appropriate method can be selected for testing according to needs.

Summary and recommendations

Accurate measurement of electroplating layer thickness is essential to ensure product quality. Choosing an appropriate test method depends on the type of coating being tested, thickness range and test accuracy requirements. In addition, international and industry standards also provide detailed test procedures and requirements to ensure the accuracy and repeatability of the test. Therefore, when conducting electroplating layer thickness tests, it is recommended to refer to relevant standards and select appropriate test methods to ensure product quality and performance.