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National Standard for Coating Viscosity Determination [Rotational Viscometer method]

Abstract: 文章介绍了涂料粘度测定的国家标准中旋转粘度计法的应用。针对触变型涂料,流出杯法因其粘度过大而不适用,此时需采用旋转粘度计。常见的旋转粘度计包括旋转桨式、同轴圆桶和锥形平板粘度计。在国家标准中,GB/T 9269-1988用于建筑涂料的粘度测定,以产生200转/分钟所需负荷表示,并可转换为克雷布斯(Krebs)单位(KU)。GB/T 9751-1988则适用于高剪切速率下的涂料粘度测定,适用于所有刷涂涂料,不论其是否具有牛顿性质。两种标准均要求测试环境温度控制在23±0.5℃。相对误差应不大于5%。文章还比较了四种涂料粘度测定方法的适用范围、测试环境条件、主要仪器和结果单位,指出流出杯法操作简便但对触变涂料不准确,而旋转粘度计法适用范围广但对环境要求较高。

The viscosity measured by the Flow Cup method for thixotropic coatings is too large, and a Rotational Viscometer is required. There are rotary paddle viscometers, coaxial drum Rotational Viscometers, conical plate viscometers, etc.

In the national standard, the method standard for measuring the viscosity of coatings by Rotational Viscometer is commonly used in GB/T 9269---1988 Determination of viscosity of architectural coatingsStoner viscometer method and GB/T 975 1-1988 Determination of viscosity of coatings at high shear rates.

GB/T 9269-1988 is suitable for the determination of the viscosity of architectural coatings, and can also be used for the determination of the viscosity of suitable coatings. It is expressed in terms of the load required to generate a speed of 200 r/min in grams (g) and can also be obtained by checking the table in GB/T 9269---1988 and the load required to generate a speed of 200 r/min and Krebs units (KU) conversion. Krebs units (KU) are a logarithmic function of the load required to generate a speed of 200 r/min and are generally used to express the viscosity used for brush and roll coatings.

In GB/T 9751-1988, the kinetic viscosity of coatings is determined at a shear rate of 5 000-20 000 s, and the shear rate should be roughly the same when comparing the viscosity of various coatings. This standard applies to all brush paints, regardless of whether they are of Newtonian nature. Rotational viscometers and conical plate viscometers can be used in this standard. For the same experimenter, the relative error between two measured values obtained by using one device in the same laboratory should not be greater than 5%.

Comparison of 4 methods for determining the viscosity of coatings

Standard number

GB/T1723-1993

GB/T6753.4-1988

GB/T9269-1988

GB/T9751-1988

Test environmental conditions

23±1°C or 25±l°C

23±0.5℃

23±0.5℃

23±0.5℃

Main instruments

Paint 1 cup, apply _4 cups

ISO Flow Cup

Stomo Viscometer

Rotational viscometer cone plate viscometer

Scope of application

Apply 1 cup of paint products for the determination of outflow time of not less than 20 s, and apply _4 cups for the determination of paint with outflow time of less than 150 s

Determination of the viscosity of Newtonian or approximately Newtonian liquid coatings

Suitable for the determination of viscosity of architectural coatings. It can also be used for the determination of viscosity of suitable coatings

Suitable for all brush coatings, regardless of whether they are incense or Newtonian properties

Result unit

S

S

Ku/g

mPa.s

Pros and cons

It is convenient to operate and clean. Easy to obtain. But for thixotropic coatings,

The viscosity measured by the Flow Cup method is too large. Viscosity values cannot be determined accurately

It has a wide range of applications, but has high requirements for temperature control in the test environment


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