Experimental equipment required for the synthesis of zirconium silicate by microemulsion method

Microemulsion is a transparent or translucent multi-phase thermodynamically stable system spontaneously formed by mixing . The Schulman method of preparing microemulsion is to mix hydrocarbon and water emulsifier evenly, drop alcohol to it, and the system suddenly becomes transparent to a certain amount of dropping to obtain microemulsion. The Shah method is to mix hydrocarbons, alcohols, and emulsifiers evenly, and add water dropwise therein until the system suddenly becomes transparent to obtain a microemulsion.

Experimental Pigments

Zirconium oxychloride, tetraethyl orthosilicate, cyclohexane, absolute ethanol, hydrochloric acid , nonylphenol polyoxyethylene, vinyl ether, n -butanol, ammonia water, acetylacetone , acetone

laboratory apparatus

Electric constant temperature Forced Air Drying Oven, high temperature box resistance furnace, low speed centrifuge, laser particle size analyzer, electric constant temperature Water Bath, electronic balance, laboratory mixer, magnetic stirrer

Experimental protocol

Mainly carry out research on the preparation of zirconium silicate by microemulsion method. The effect of calcination temperature on the preparation of zirconium silicate powder by microemulsion method was discussed .

Calcination temperatures are: 1000°C, 1100°C, 1200°C, 1300C