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What is an indentation peel test?

Abstract: 这篇文章探讨了压痕剥离测试的原理及其在评估涂层附着力方面的应用。该测试通过将针状压头垂直压入涂层表面来测量涂层与基体之间的附着力。在测试过程中,大部分变形发生在涂层内部,但界面处也可能出现脱粘现象。通过计算剥离力矩,可以评估薄膜在压痕点附近的分层能力,特别适用于监测薄涂层的脱粘面积。除了传统的渗透型压头,其他形状的压头也能有效应用于此测试,其中60°角的圆锥形压头被证明在计算粘附值时尤其有效。该测试方法的优点包括能够提供粘结强度的绝对值及在特定载荷条件下涂层和基材之间连接的耐久性信息。

If the needle-shaped indenter is pressed vertically into the coating surface, the coating is bonded to the almost indeformable substrate, and most of the deformation will occur inside the film, but there will also be some debonding at the interface.

From this, as shown in Figure 6.10, the peel torque can be calculated, which can be used as a measure of the ability of the film to withstand delamination near the indentation point. This is convenient, especially for thin coatings, to monitor the gradually increasing debonding Areas and optics can lead to evaluations based on, for example, Newton's rings, and clear coatings.

It is not necessary to limit the scope of the indentation test to the use of penetration against the coating. Other typical shapes of indenters have also been used with success. The results show that, considering the boundary conditions on the interface, as a basis for calculating the adhesion value, a good method is to use a cone with an angle of 60° as the indenter. An important advantage of this qualification test is that it can obtain the absolute value of the bond strength, As well as information on the durability of the connection between the coating and the substrate under specific loading conditions.

Schematic diagram of the indentation process for measuring polymer-substrate interface adhesion

Principles of the indentation process for measuring adhesion at the polymer-substrate interface


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