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Dip coating process and dip coating machine

Abstract: 本文介绍了浸涂工艺及其在浸涂机上的应用,强调了其在制造薄膜方面的简单性和有效性。浸涂技术因其设计简单、成本低廉及能生产高均匀性和纳米级粗糙度薄膜的能力而受到广泛应用。文章指出,为了实现薄膜的高质量生产,必须优化参数如退出速度,并密切监测包括温度、气流和清洁度在内的大气因素。浸涂过程包括五个主要步骤:浸没、住宅、退出、烘干和可选的固化。重点分析了退出和干燥阶段在薄膜厚度控制中的关键作用,介绍了粘性流动、排水和毛细管状态的影响,并提出了一个综合方程来解释不同速度范围内的厚度与提取速度关系。通过对浸涂过程的各个阶段的理解,可以有效控制最终薄膜的厚度和质量。

Dip coating is a simple yet effective technique widely used in manufacturing in different industries. During research and development, it has become an important coating method for the manufacture of thin films using a dedicated dip coater. When the process is optimized, dip coating can be used to produce highly uniform films. Remember: Critical factors such as film thickness can be easily controlled.

One of the advantages of dip coating compared to other processing techniques is its simplicity of design. It is inexpensive to set up and maintain, and can produce films with extremely high uniformity and nanoscale roughness.

Dip coating is a relatively simple technique. However, in order to achieve a greater degree of control when coating substrates, it is important to understand what factors can affect your results. In order to make high-quality films, parameters such as exit speed need to be optimized. Atmospheric factors including temperature, air flow and cleanliness also have a large impact on film quality and need to be closely monitored during dip coating. As with other methods, flaws can occur, but by knowing the root cause, it is relatively easy to find the source of the problem and take appropriate action.

Dip coating involves the deposition of a liquid film by the precise and controlled removal of the substrate from solution using a dip coater. The dip coating process requires a minimum of four distinct steps (or stages), followed by an optional fifth curing step:

  • immersion

  • Residential

  • quit

  • drying

  • curing (optional)

All these stages are required in the dip coating process. However, the two critical points that determine the properties of the deposited film are the extraction and drying stages. During these stages, the final film thickness is determined by the interplay between entrainment, drainage and film drying:

  • viscous flow

  • drainage

  • Capillary

Transitions between each of these protocols occurred at different values of extraction speed and solution viscosity. The combination of the three coating schemes ultimately determines the "thickness versus withdrawal speed" behavior of the film. By summing the contributions of the drained state and the capillary state, an equation can be obtained that accounts for the thickness extraction velocity relationship over a wide range of velocities. This also allows us to determine the smallest possible thickness that the solution can be applied to.

Lower the substrate into the solution bath until it is mostly or completely submerged. A short delay occurs before the substrate is removed. During withdrawal, a thin layer of solution remains on the surface of the substrate. Once fully withdrawn, the liquid in the film begins to evaporate and leaves a dry film. For some materials, a further curing step can be performed to force chemical or physical changes in the deposited material.

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