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Laboratory Coating Machine Case | Sewage Treatment Flat Membrane/Vinylidene Fluoride PVDF Preparation

Abstract: 文章介绍了在实验室使用涂膜机制备污水处理用平板膜的案例,特别是基于聚偏氟乙烯(PVDF)材料的膜。随着化工和冶金行业的发展,对重金属污水处理的需求增加,本实验旨在提高污水处理效率。制备过程中使用了浸没沉淀相转化法,将PVDF粉末与溶剂和添加剂混合,在控制的实验室条件下进行膜制备。具体步骤包括搅拌、加热、超声波处理、刮膜和水浴凝固等。文章还讨论了选择涂膜机的关键点,如基材为玻璃板、刮刀涂布和无需加热功能。推荐使用可调刮刀的刮刀式涂膜机,具备高精度和多功能,以满足不同的实验需求。

With the rapid development of the chemical and metallurgical industries, the treatment of heavy metal sewage is also a social and environmental issue that has attracted more and more attention. Therefore, many scientific researchers are constantly studying new technologies to improve the efficiency of sewage treatment. The preparation case of the membrane coating machine in this laboratory is the preparation of a flat filter membrane for sewage treatment, a flat ultrafiltration separation membrane with adsorption function for heavy metal ions prepared by compounding polyvinylidene fluoride membrane material and attapulgite. Used to improve the efficiency of sewage treatment.

Laboratory film coating machine case | Sewage treatment flat film / vinylidene fluoride PVDF preparation picture 1

The specific operation method of extracting papers is as follows:

The modified ultrafiltration membrane used in this experiment is a laboratory-made membrane. The modified membrane uses polyvinylidene fluoride (PVDF) as the base membrane material, and the preparation method is the immersion precipitation phase inversion method. At room temperature in the laboratory, put a certain mass ratio of PVDF powder in a beaker, pour a certain volume of N, N-dimethyl ethylene glue (DMAc) solution, stir well, and pour it into the PVDF casting solution Add a certain mass ratio of polyvinylpyrrolidone (PVP) and graphene oxide, stir evenly, place in a constant temperature Water Bath at 40C for heating and stirring in a Water Bath for 2, and perform ultrasonic treatment for 1h at a Water Bath temperature of 40C, and then let stand for 24h Let it fully mature and defoam. Control the speed of 0.839m/min on the film coating machine to scrape the film on the glass plate, control the film thickness to about 0.2mm, and then control the glass plate to enter the water at a direction of 30°~60°, and spread the casting liquid The glass plate is quickly immersed in deionized water, and after the Water Bath is solidified to form a film, the new film is separated from the glass plate. The prepared new membrane needs to be rinsed with deionized water, and then soaked in deionized water for more than 24 hours. These processes are mainly to remove the residual solvent in the membrane pores.

Laboratory film coating machine case | Sewage treatment flat film / vinylidene fluoride PVDF preparation picture 2

From the information of the preparation experiment, we can see several key points in the selection of the film coating machine. First, the base material is on a glass plate, so there is no need for a vacuum adsorption plate; second, a scraper should be used for scraping coating , the thickness of the scraped film is about 200 μm, which is relatively thick, and can be prepared with an adjustable scraper ; third, this experiment does not require a heating function;

According to the requirements of the experiment, we technically recommend the scraper integrated film coating machine to the customer. The scraper is an adjustable film thickness scraper, which can be freely adjusted from 0 to 10mm to meet the experimental needs of more film thickness. The specific parameters are as follows:

Membrane Proofing- Membrane
Laboratory film coating machine case | Sewage treatment flat film / vinylidene fluoride PVDF preparation picture 3Domestic TBJ-B1 scraper coating testing machine
Specification parameters: coating precision ±0.003mm, coating thickness range 0.01~10mm, coating speed 2~200mm/s, coating width 300*400mm, digital display of coating time, different speeds, distance precision control, scraper Length 400MM Material/stainless steel, main engine power supply 220V 50HZ, external dimensions 626*410*520mm, net weight 45KG, speed control stepless speed change, bottom plate material glass plate, optional accessories leakage tank, substrate fixing fixture, fine-tuning level height support feet Device, glass plate, silicone pad and weight (for the application of uneven thickness of coating substrate), coating film width control baffle, customizable function air jet system device, UV solid containing device, automatic ink filling system

The above parameters are for reference only. According to different actual experiments, with further targeted selection of appropriate configuration, it can communicate with the North and South tide technology.

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