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Adhesion Test of Anti-Fog Coatings with Paint Film Scratch

Author: 张世贤
Source: 湖北大学
Abstract: 这篇文章描述了使用漆膜划格器测试防雾涂层附着力的方法。首先,将固化后的PET薄膜裁剪成3x3 cm的样品用于水接触角和透光率雾度测试,10x30 cm的样品用于附着力、涂膜柔韧性和耐湿磨性能测试。根据ASTM D3359标准,使用带有11个刀刃的划格器在样品表面进行切割。确保切割过程中的角度和压力均匀,并使刀刃完全切入涂层。之后,用软毛刷清除漆膜粉末,贴上600型3M胶带,进行剥离测试。根据漆膜的脱落情况,样品被评定为5B、4B、3B、2B、1B或0B级,表示附着力的强弱。每个样品在不同区域至少重复测试一次。

After the coating is cured, use scissors to cut the PET film into 3x3cm samples for water contact angle and light transmittance haze test; cut the PET film into 10>x30cm samples for adhesion, coating film flexibility, wet abrasion resistance Performance testing .

Adhesion test of anti-fog coating with a paint cross-hatch with Figure 1

Adhesion tests were performed on the samples using the cross-hatch standard in ASTM D3359. Cut the surface of the sample with a scribe with 11 blades and a distance between blades of 1 mm under sufficient lighting conditions. During the cutting process , all cutting angles should be consistent, the cutting pressure should be uniform, and it is necessary to ensure that the blade completely cuts the coating and touches the PET substrate. Carry out a second cut of the sample in a direction perpendicular to the direction of the first cut. After cutting, brush off the paint film , paste it on the cross grid on the paint film with 600-type 3M adhesive tape, and flatten it with your fingers to ensure good contact. After 30s, pull down the tape slowly at an angle of 180 degrees at a constant speed, and check the peeling of the paint film from the substrate in the grid area. The knife edge is smooth and has no falling off, which is grade 5B; the number of missing grids is less than 5 grids, which is grade 4B; the number of falling grids is 5-15 grids, which is grade 3B ; 35-65 grids are recorded as IB grade; the number of missing grids is more than 65 grids is recorded as 0B grade. The small cell with a fall-off area greater than 50% is calculated as l cell. Each sample was replicated at least in different regions.


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